My first Bionicle set was Matoro from the Toa Mahri, and my bio basically explains that whole story 
I still remember the day, and every now and then I pass by the school that it all started ;-;
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My first set was the Nuhvok.
I got Thok, Vezok, and Reidak as birthday presents in 2006, and with the form on the back of one of their instructions I got my first Lego Magazine subscription. (And also my first Bionicle Comic).
Kongu Mahri. -Said nobody else, ever.
Hey, Kongu Mahri was my first Toa Mahri. So there.
Metru Matau, followed closely by Metru Nuju.
Very first: Mctoran Onepu
First actual set: Thanok(2002)
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My first Bionicle was Lewa Mata.
Turaga Whenua. It came free with the old Lego Adventures magazine 
Fun side note: I hated Bionicle until I got that. Idiot ten year old for you there. Then I got Whenua and bought everything
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Mine was Dalu from 2006. I was eight at the time. Good memoriesâŚ
I got her in the Brickmaster program that year. Best thing I ever got out of that.
Werenât there a whole bunch of exclusive models/polybags as part of that program?
Yes, one every two months, and Dalu is the only one I can remember. Wait⌠no, there was a little Harry Potter bus thingy. I got two of those.
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That makes waves and waves of bittersweet nostalgia well up within me.
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My first set was nuuvak-kal, which I had to share with my bro. My first toa set was toa mahri jaller.
My first was Kopaka Mata.
my first bionicle set was kalmah and jaller inika from toys r us
You know, I donât remember my first set (I was around 5), but I know it was a Toa Mata. I often claim itâs Kopaka but thatâs only because I wound up owning around three of him at one point. Whoever it was, I remember getting mad because it wasnât Tahu and heâs the one I wanted the most.